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Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
Zakup książki
X-Ray Structure Determination, George H. Stout
- Język
- Rok wydania
- 1989
- Oprawa
- (twarda)
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- Tytuł
- X-Ray Structure Determination
- Podtytuł
- A Practical Guide, 2nd Edition
- Język
- angielski
- Autorzy
- George H. Stout
- Wydawca
- Wiley-Interscience
- Rok wydania
- 1989
- Oprawa
- twarda
- Liczba stron
- 480
- ISBN10
- 0471607118
- ISBN13
- 9780471607113
- Seria
- Opis
- Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.